data.org

plt.figure(1)
plt.plot(1, 2)
plt.xlabel(u'我是横坐标')
plt.ylabel(u'我是纵坐标')
plt.show()

• $\frac{V × M × 100.8 × 1000}{V_w}$
• \[C_EDTA = 0.0089 \text{mol}/L\]
• \[V_L50 = 50 ml = 0.05L\]
• X: 钙离子浓度(以 $CaCO_3$ 计), mg/L;
• V: 滴定时EDTA标准溶液消耗的体积, mL;
• M = 0.0089: EDTA标准溶液的浓度, mol/L;
• $V_m = 50$: 水样的体积, mL;
• 100.8: $CaCO₃$ 的摩尔质量, g/mol.
• result = 17.9424 * V
• result2 = 16.10784 * V

L50 2g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

0.5h

7.79

3.9434

0.16

0.30

0.23

8.00

4.127

----------------+-----------+----------+----------+--------+--------+--------------+

1h

7.45

4.0125

0.48

0.46

0.47

0.27

8.433

----------------+-----------+----------+----------+--------+--------+--------------+

2h

6.6

3.9806

0.51

0.58

0.55

9.79

9.868

----------------+-----------+----------+----------+--------+--------+--------------+

3h

7.04

3.9820

0.95

0.90

0.93

9.84

16.686

----------------+-----------+----------+----------+--------+--------+--------------+

6h

7.56

3.9874

1.85

1.91

1.88

10.22

33.732

----------------+-----------+----------+----------+--------+--------+--------------+

8h

7.54

3.9817

2.22

2.21

2.22

10.32

39.832

----------------+-----------+----------+----------+--------+--------+--------------+

10h

7.58

3.9999

2.31

2.30

2.31

10.34

41.447

----------------+-----------+----------+----------+--------+--------+--------------+

12h

7.21

4.0511

2.50

2.53

2.52

10.52

45.215

----------------+-----------+----------+----------+--------+--------+--------------+

16h

7.71

4.0014

2.85

2.88

2.87

10.46

51.494

----------------+-----------+----------+----------+--------+--------+--------------+

20h

7.98

4.0470

3.32

3.38

3.35

10.50

59.107

----------------+-----------+----------+----------+--------+--------+--------------+

24h

6.64

4.0410

3.33

3.55

3.44

10.61

61.722

----------------+-----------+----------+----------+--------+--------+--------------+

28h

8.29

4.0133

4.01

3.98

4.00

10.67

71.769

----------------+-----------+----------+----------+--------+--------+--------------+

40h

7.54

4.0077

4.47

4.57

4.52

10.76

81.100

----------------+-----------+----------+----------+--------+--------+--------------+

52h

7.71

4.0181

4.39

4.40

4.40

10.74

78.946

----------------+-----------+----------+----------+--------+--------+--------------+

64h

7.85

3.9628

4.62

4.80

4.71

10.84

84.509

----------------+-----------+----------+----------+--------+--------+--------------+

88h

7.77

3.9832

5.94

5.90

5.92

10.96

106.219

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.46

3.9474

7.30

7.19

7.25

11.11

130.082

----------------+-----------+----------+----------+--------+--------+--------------+

192h

7.54

4.0262

7.50

7.81

7.66

11.14

137.439

----------------+-----------+----------+----------+--------+--------+--------------+

280h

7.27

4.0021

7.65

7.70

7.68

11.67

123.7082

----------------+-----------+----------+----------+--------+--------+--------------+

L50 3g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.23

6.0225

8.17

8.22

8.20

11.06

147.128

----------------+-----------+----------+----------+--------+--------+--------------+

L50 4g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.21

7.9501

9.51

9.50

9.51

11.12

170.632

----------------+-----------+----------+----------+--------+--------+--------------+

L50 5g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

3h

7.72

10.0179

2.07

2.27

2.17

10.27

38.935

----------------+-----------+----------+----------+--------+--------+--------------+

16h

7.53

9.9756

6.47

6.39

6.43

10.78

115.370

----------------+-----------+----------+----------+--------+--------+--------------+

40h

7.34

9.9869

9.43

9.30

9.37

10.95

168.120

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.73

9.9246

9.33

9.35

9.34

11.13

167.582

----------------+-----------+----------+----------+--------+--------+--------------+

L50 pH=4.13:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

4.13

4.0266

6.20

6.05

6.13

10.83

109.987

----------------+-----------+----------+----------+--------+--------+--------------+

L50 pH=2.09 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

2.09

3.9901

4.40

5.18

4.79

9.19

85.944

----------------+-----------+----------+----------+--------+--------+--------------+

L50 pH=9 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

9.97

3.9855

5.78

5.80

5.79

10.97

103.886

----------------+-----------+----------+----------+--------+--------+--------------+

L60 2g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

0.5h

7.68

3.9229

0.12

0.12

0.12

9.52

2.153

----------------+-----------+----------+----------+--------+--------+--------------+

1h

7.61

4.0753

0.47

0.51

0.49

9.66

8.792

----------------+-----------+----------+----------+--------+--------+--------------+

2h

7.78

3.9807

0.71

0.70

0.71

10.18

12.739

----------------+-----------+----------+----------+--------+--------+--------------+

3h

7.39

3.9222

0.70

0.81

0.76

10.36

13.636

----------------+-----------+----------+----------+--------+--------+--------------+

6h

7.34

4.0430

0.92

0.91

0.92

10.38

16.507

----------------+-----------+----------+----------+--------+--------+--------------+

8h

7.40

3.9801

1.27

1.37

1.32

10.71

23.684

----------------+-----------+----------+----------+--------+--------+--------------+

10h

7.71

4.0198

1.80

1.79

1.80

10.86

32.296

----------------+-----------+----------+----------+--------+--------+--------------+

12h

7.19

3.9577

1.80

1.62

1.71

10.74

30.681

----------------+-----------+----------+----------+--------+--------+--------------+

16h

6.88

4.0333

1.84

1.86

1.85

10.79

32.193

----------------+-----------+----------+----------+--------+--------+--------------+

20h

7.32

3.9780

2.46

2.32

2.39

10.82

42.882

----------------+-----------+----------+----------+--------+--------+--------------+

24h

7.41

4.0010

2.58

2.56

2.57

10.95

46.112

----------------+-----------+----------+----------+--------+--------+--------------+

32h

7.34

4.0132

2.89

2.87

2.88

11.00

51.674

----------------+-----------+----------+----------+--------+--------+--------------+

40h

7.65

3.9898

3.03

3.12

3.08

11.04

55.263

----------------+-----------+----------+----------+--------+--------+--------------+

52h

7.86

3.9730

3.60

3.76

3.68

11.00

66.028

----------------+-----------+----------+----------+--------+--------+--------------+

64h

7.45

4.0198

3.90

4.10

4.00

11.15

71.770

----------------+-----------+----------+----------+--------+--------+--------------+

88h

7.49

3.9688

4.20

4.20

4.20

11.11

75.358

----------------+-----------+----------+----------+--------+--------+--------------+

112h

7.45

3.9403

4.70

4.99

4.86

11.14

87.200

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.48

3.9420

4.70

4.99

4.86

11.14

92.205

----------------+-----------+----------+----------+--------+--------+--------------+

192h

7.41

3.9268

5.98

5.70

5.84

11.43

104.783

----------------+-----------+----------+----------+--------+--------+--------------+

280h

7.29

4.0212

5.90

5.93

5.92

11.98

95.3584

----------------+-----------+----------+----------+--------+--------+--------------+

L60 3g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.42

6.0103

5.90

5.80

5.85

11.38

104.963

----------------+-----------+----------+----------+--------+--------+--------------+

L60 5g/100ml 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

7.31

10.0125

7.30

7.40

7.35

11.45

131.877

----------------+-----------+----------+----------+--------+--------+--------------+

L60 pH=1.98:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

1.98

3.9951

7.80

8.65

8.23

8.20

147.666

----------------+-----------+----------+----------+--------+--------+--------------+

L60 pH=3.93:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

3.93

4.0336

5.50

5.40

5.45

11.18

97.786

----------------+-----------+----------+----------+--------+--------+--------------+

L60 pH=9 初始pH为超纯水:

----------------+-----------+----------+----------+--------+--------+--------------+

time

pH

ceramsites

edta 1(ml)

edta 2(ml)

average

pH(end)

result(mg/L)

----------------+-----------+----------+----------+--------+--------+--------------+

136h

9.88

4.0518

4.95

5.00

4.98

11.14

89.353

----------------+-----------+----------+----------+--------+--------+--------------+

蠕动泵流速

• 0.1转速: 240ml/24h 10
• 0.2转速: 15.5h 330ml 21.29
• 0.3转速: 410ml 13:23H 30.635
• 0.4转速: 590ml 13:23H 44.08
• 0.5转速: 870ml 16::17 53.43
• 0.6转速: 1060ml 16::17 65.1
• 0.7 550 7:34 72.684
• 0.8 680 7:34 89.864
• 0.9 1160 11:34 100.282
• 1.0: 560 112
• 1.1: 620 5h 124

To Ask

1. 原料配比具体指哪些 强度, 空隙结构影响因素

动态

4号

35min 9.96 1:23 10.05 2:00 10.16 2:46 10.24 4.05 4:30 10.50 5:00 10.59 11 9:00 10.72 16.8 11:00 10.87 18.80 12:00 10.89 19.80 24:00 10.97 23.4 28:00 10.95 26.40 37:00 11.03 24.16 47:00 11.10 22.80 78:00 10.95 16.96

123:00 11.07 9.8 155:00 11.10 8.5 195:30 11.50 4.8 219:00 11.67 6.30 270:00 11.66 5.70

L60

35min 10.63 1:23 10.83 2:00 10.84 3.0 3:00 10.99 4.20 4:30 11.11 5:00 11.13 5.62 9:00 11.26 7.03 11:00 11.34 8.17 12:00 11.39 8.22 24:00 11.21 7.28 28:00 11.27 7.38 37:00 11.35 8.02 47:00 11.40 7.84 78:00 11.20 7.20

123:00 11.28 4.60 155:00 11.33 5.20 195:30 11.72 7.50 219:00 11.84 6.25 270:00 11.85 5.60

2.4970g/1000ml = 0.02477mol/1000ml = 0.02477mol/l = 0.00002477mol/ml 3.4ml 1ml = 10mg 3.9945g/300ml

0.00002477mol * 336.21 = 0.0083279217 g / 3.1ml = 0.00799

出图

静态

时间变量

释钙

pH

投加量变量

4号 5g/100ml

释钙

pH

释钙

pH

pH变量

释钙

pH

动态

释钙

pH

实验装置图片