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[1]DPh-NDT_1.CIF
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#------------------------------------------------------------------------------
data__DPh-anti-NDT
#------------------------------------------------------------------------------
# CHEMICAL DATA
_chemical_formula_sum 'C26 H16 S2 '
_chemical_formula_moiety 'C26 H16 S2 '
_chemical_formula_weight 392.53
_chemical_melting_point ?
#------------------------------------------------------------------------------
# CRYSTAL DATA
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 1 21/n 1'
_symmetry_Int_Tables_number 14
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
1/2-x,1/2+y,1/2-z
-x,-y,-z
1/2+x,1/2-y,1/2+z
_cell_length_a 5.922(10)
_cell_length_b 7.60(1)
_cell_length_c 40.63(7)
_cell_angle_alpha 90.000(6)
_cell_angle_beta 93.753(6)
_cell_angle_gamma 90.000(6)
_cell_volume 1823.6(4)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 2699
_cell_measurement_theta_min 3.0
_cell_measurement_theta_max 27.5
_cell_measurement_temperature 293.1
#------------------------------------------------------------------------------
_exptl_crystal_description 'Platelet'
_exptl_crystal_colour 'Yellow'
_exptl_crystal_size_max 0.600
_exptl_crystal_size_mid 0.500
_exptl_crystal_size_min 0.100
_exptl_crystal_size_rad ?
_exptl_crystal_density_diffrn 1.430
_exptl_crystal_density_meas ?
_exptl_crystal_density_method 'not measured'
_exptl_absorpt_coefficient_mu 0.301
_exptl_absorpt_correction_type none
#------------------------------------------------------------------------------
# EXPERIMENTAL DATA
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.7107
_diffrn_measurement_device_type 'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method \w
_diffrn_detector_area_resol_mean 14.71
_diffrn_reflns_number 10967
_diffrn_reflns_av_R_equivalents 0.103
_diffrn_reflns_theta_min ?
_diffrn_reflns_theta_max 27.49
_diffrn_reflns_limit_h_min -7
_diffrn_reflns_limit_h_max 3
_diffrn_reflns_limit_k_min -9
_diffrn_reflns_limit_k_max 8
_diffrn_reflns_limit_l_min -52
_diffrn_reflns_limit_l_max 52
#------------------------------------------------------------------------------
# REFINEMENT DATA
_refine_special_details
;
Refinement using reflections with F^2^ > 2.0 sigma(F^2^). The weighted
R-factor (wR) and goodness of fit (S) are based on F^2^. R-factor (gt) are
based on F. The threshold expression of F^2^ > 2.0 sigma(F^2^) is used only
for calculating R-factor (gt).
;
_reflns_number_total 3799
_reflns_number_gt 2229
_reflns_threshold_expression >2.0sigma(I)
_refine_ls_structure_factor_coef Fsqd
_refine_ls_R_factor_gt 0.0949
_refine_ls_wR_factor_ref 0.3005
_refine_ls_hydrogen_treatment noref
_refine_ls_number_reflns 2229
_refine_ls_number_parameters 253
_refine_ls_goodness_of_fit_ref 1.116
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.1304P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_shift/su_max -0.0010
_refine_ls_extinction_method SHELXL
_refine_ls_extinction_coef 0.0000
_refine_ls_extinction_expression
'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^'
_refine_diff_density_max 0.47
_refine_diff_density_min -0.60
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
'C' 'C' 0.003 0.002
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
'H' 'H' 0.000 0.000
;International Tables for Crystallography
(1992, Vol. C, Table 6.1.1.4)
;
'S' 'S' 0.125 0.123
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.4)
;
#------------------------------------------------------------------------------
# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
S(1) S 0.3769(2) 0.1581(2) 0.14561(3) 0.0496(4) Uani 0.81 d P . .
S(2) S 0.6245(2) -0.0132(2) 0.35163(3) 0.0492(4) Uani 0.81 d P . .
C(1) C 0.6333(7) 0.0657(4) 0.1345(1) 0.0436(9) Uani 1.00 d . . .
C(2) C 0.8017(7) -0.0123(4) 0.16172(8) 0.072(1) Uani 1.50 d P . .
C(3) C 0.6643(6) 0.0290(4) 0.1931(1) 0.0415(9) Uani 1.00 d . . .
C(4) C 0.7427(6) -0.0099(4) 0.2251(1) 0.0413(9) Uani 1.00 d . . .
C(5) C 0.6111(6) 0.0327(4) 0.2519(1) 0.0373(9) Uani 1.00 d . . .
C(6) C 0.6888(7) -0.0066(4) 0.2851(1) 0.0420(9) Uani 1.00 d . . .
C(7) C 0.5561(7) 0.0344(4) 0.3104(1) 0.0440(9) Uani 1.00 d . . .
C(8) C 0.3684(7) 0.0775(4) 0.3627(1) 0.0427(9) Uani 1.00 d . . .
C(9) C 0.2001(7) 0.1584(4) 0.33530(8) 0.073(1) Uani 1.50 d P . .
C(10) C 0.3409(7) 0.1206(4) 0.3045(1) 0.0436(9) Uani 1.00 d . . .
C(11) C 0.2622(7) 0.1614(4) 0.2724(1) 0.0431(9) Uani 1.00 d . . .
C(12) C 0.3941(6) 0.1190(4) 0.2455(1) 0.0388(9) Uani 1.00 d . . .
C(13) C 0.3152(6) 0.1591(4) 0.2123(1) 0.0415(9) Uani 1.00 d . . .
C(14) C 0.4480(7) 0.1152(4) 0.1870(1) 0.0433(9) Uani 1.00 d . . .
C(15) C 0.6822(7) 0.0636(4) 0.0998(1) 0.0448(9) Uani 1.00 d . . .
C(16) C 0.5349(8) 0.1396(5) 0.0754(1) 0.056(1) Uani 1.00 d . . .
C(17) C 0.5823(10) 0.1374(6) 0.0426(1) 0.067(1) Uani 1.00 d . . .
C(18) C 0.7764(10) 0.0570(6) 0.0331(1) 0.069(1) Uani 1.00 d . . .
C(19) C 0.9264(9) -0.0201(6) 0.0569(1) 0.064(1) Uani 1.00 d . . .
C(20) C 0.8813(8) -0.0169(5) 0.0897(1) 0.053(1) Uani 1.00 d . . .
C(21) C 0.3153(7) 0.0727(4) 0.3970(1) 0.0436(9) Uani 1.00 d . . .
C(22) C 0.4569(8) -0.0147(5) 0.4213(1) 0.057(1) Uani 1.00 d . . .
C(23) C 0.4044(10) -0.0179(6) 0.4537(1) 0.066(1) Uani 1.00 d . . .
C(24) C 0.2104(9) 0.0652(6) 0.4637(1) 0.062(1) Uani 1.00 d . . .
C(25) C 0.0697(9) 0.1485(6) 0.4405(1) 0.063(1) Uani 1.00 d . . .
C(26) C 0.1169(8) 0.1523(5) 0.4076(1) 0.054(1) Uani 1.00 d . . .
H(1) H 0.9444 -0.0689 0.1600 0.0716 Uiso 1.00 calc . . .
H(2) H 0.8874 -0.0649 0.2292 0.0445 Uiso 1.00 calc . . .
H(3) H 0.8331 -0.0613 0.2891 0.0461 Uiso 1.00 calc . . .
H(4) H 0.0574 0.2165 0.3371 0.0759 Uiso 1.00 calc . . .
H(5) H 0.1207 0.2215 0.2685 0.0480 Uiso 1.00 calc . . .
H(6) H 0.1717 0.2169 0.2083 0.0459 Uiso 1.00 calc . . .
H(7) H 0.3996 0.1969 0.0818 0.0618 Uiso 1.00 calc . . .
H(8) H 0.4813 0.1946 0.0265 0.0740 Uiso 1.00 calc . . .
H(9) H 0.8034 0.0502 0.0101 0.0739 Uiso 1.00 calc . . .
H(10) H 1.0632 -0.0751 0.0509 0.0708 Uiso 1.00 calc . . .
H(11) H 0.9836 -0.0702 0.1055 0.0590 Uiso 1.00 calc . . .
H(12) H 0.5915 -0.0725 0.4151 0.0639 Uiso 1.00 calc . . .
H(13) H 0.4985 -0.0854 0.4696 0.0699 Uiso 1.00 calc . . .
H(14) H 0.1750 0.0642 0.4869 0.0705 Uiso 1.00 calc . . .
H(15) H -0.0670 0.2061 0.4466 0.0701 Uiso 1.00 calc . . .
H(16) H 0.0150 0.2107 0.3920 0.0598 Uiso 1.00 calc . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
S(1) 0.0437(8) 0.0556(7) 0.0495(9) 0.0062(5) 0.0030(6) 0.0015(5)
S(2) 0.0428(8) 0.0546(7) 0.0502(9) 0.0054(5) 0.0036(6) 0.0003(5)
C(1) 0.043(2) 0.036(2) 0.052(2) -0.002(1) -0.001(2) -0.000(1)
C(2) 0.110(3) 0.060(2) 0.046(2) -0.035(2) 0.002(2) -0.000(1)
C(3) 0.036(2) 0.036(2) 0.053(3) -0.001(1) 0.004(2) -0.003(1)
C(4) 0.027(2) 0.038(2) 0.060(3) -0.000(1) 0.007(2) -0.001(2)
C(5) 0.024(2) 0.034(2) 0.053(2) 0.001(1) -0.003(2) -0.001(1)
C(6) 0.036(2) 0.039(2) 0.050(2) 0.002(1) -0.001(2) 0.002(1)
C(7) 0.038(2) 0.041(2) 0.052(3) -0.005(2) -0.004(2) -0.001(2)
C(8) 0.040(2) 0.035(2) 0.052(3) 0.000(1) 0.001(2) 0.000(1)
C(9) 0.113(3) 0.062(2) 0.045(2) -0.039(2) 0.006(2) -0.003(1)
C(10) 0.040(2) 0.038(2) 0.054(3) -0.004(1) 0.010(2) -0.005(2)
C(11) 0.034(2) 0.036(2) 0.060(3) -0.000(1) 0.006(2) -0.006(2)
C(12) 0.028(2) 0.035(2) 0.053(2) -0.002(1) 0.001(2) -0.003(1)
C(13) 0.029(2) 0.039(2) 0.056(3) 0.001(1) -0.001(2) 0.000(1)
C(14) 0.039(2) 0.041(2) 0.049(2) -0.003(1) -0.001(2) -0.001(2)
C(15) 0.042(2) 0.039(2) 0.054(3) -0.000(2) 0.004(2) 0.001(2)
C(16) 0.046(3) 0.058(2) 0.063(3) 0.006(2) 0.010(2) 0.007(2)
C(17) 0.076(4) 0.073(3) 0.051(3) 0.008(2) 0.001(3) 0.008(2)
C(18) 0.072(4) 0.076(3) 0.060(3) 0.002(3) 0.016(3) -0.001(2)
C(19) 0.061(3) 0.072(3) 0.061(3) 0.012(2) 0.015(3) -0.002(2)
C(20) 0.048(3) 0.054(2) 0.056(3) 0.005(2) 0.005(2) 0.001(2)
C(21) 0.040(2) 0.040(2) 0.051(3) -0.003(1) -0.000(2) -0.003(2)
C(22) 0.054(3) 0.060(2) 0.056(3) 0.007(2) 0.002(2) -0.002(2)
C(23) 0.074(4) 0.075(3) 0.048(3) 0.005(2) -0.008(3) 0.005(2)
C(24) 0.069(3) 0.069(3) 0.050(3) -0.003(2) 0.011(2) -0.005(2)
C(25) 0.056(3) 0.075(3) 0.058(3) 0.001(2) 0.015(2) -0.007(2)
C(26) 0.040(2) 0.062(2) 0.060(3) 0.007(2) 0.005(2) -0.005(2)
#------------------------------------------------------------------------------
_computing_data_collection 'CRYSTALCLEAR'
_computing_cell_refinement 'CRYSTALCLEAR'
_computing_data_reduction 'teXsan Ver. 1.11'
_computing_structure_solution SIR92
_computing_structure_refinement 'SHELXL97'
_computing_publication_material 'teXsan Ver. 1.11'
_computing_molecular_graphics ?
#------------------------------------------------------------------------------
_geom_special_details
;
?
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S(1) C(1) 1.759(5) . . yes
S(1) C(14) 1.737(4) . . yes
S(2) C(7) 1.735(4) . . yes
S(2) C(8) 1.751(5) . . yes
C(1) C(2) 1.558(5) . . yes
C(1) C(15) 1.456(6) . . yes
C(2) C(3) 1.587(6) . . yes
C(3) C(4) 1.384(6) . . yes
C(3) C(14) 1.445(6) . . yes
C(4) C(5) 1.418(6) . . yes
C(5) C(6) 1.430(6) . . yes
C(5) C(12) 1.451(5) . . yes
C(6) C(7) 1.369(6) . . yes
C(7) C(10) 1.439(6) . . yes
C(8) C(9) 1.570(5) . . yes
C(8) C(21) 1.448(6) . . yes
C(9) C(10) 1.576(6) . . yes
C(10) C(11) 1.391(6) . . yes
C(11) C(12) 1.421(6) . . yes
C(12) C(13) 1.430(6) . . yes
C(13) C(14) 1.376(6) . . yes
C(15) C(16) 1.403(6) . . yes
C(15) C(20) 1.413(6) . . yes
C(16) C(17) 1.378(7) . . yes
C(17) C(18) 1.379(8) . . yes
C(18) C(19) 1.399(7) . . yes
C(19) C(20) 1.373(7) . . yes
C(21) C(22) 1.418(6) . . yes
C(21) C(26) 1.414(6) . . yes
C(22) C(23) 1.375(7) . . yes
C(23) C(24) 1.393(8) . . yes
C(24) C(25) 1.369(7) . . yes
C(25) C(26) 1.385(7) . . yes
#------------------------------------------------------------------------------
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C(1) S(1) C(14) 90.9(2) . . . yes
C(7) S(2) C(8) 90.8(2) . . . yes
S(1) C(1) C(2) 119.4(3) . . . yes
S(1) C(1) C(15) 118.9(3) . . . yes
C(2) C(1) C(15) 121.7(3) . . . yes
C(1) C(2) C(3) 99.1(3) . . . yes
C(2) C(3) C(4) 123.6(3) . . . yes
C(2) C(3) C(14) 116.6(3) . . . yes
C(4) C(3) C(14) 119.8(4) . . . yes
C(3) C(4) C(5) 120.4(3) . . . yes
C(4) C(5) C(6) 121.3(3) . . . yes
C(4) C(5) C(12) 119.3(4) . . . yes
C(6) C(5) C(12) 119.4(4) . . . yes
C(5) C(6) C(7) 119.7(3) . . . yes
S(2) C(7) C(6) 124.5(3) . . . yes
S(2) C(7) C(10) 113.9(3) . . . yes
C(6) C(7) C(10) 121.6(4) . . . yes
S(2) C(8) C(9) 119.5(3) . . . yes
S(2) C(8) C(21) 118.9(3) . . . yes
C(9) C(8) C(21) 121.6(3) . . . yes
C(8) C(9) C(10) 98.5(3) . . . yes
C(7) C(10) C(9) 117.3(3) . . . yes
C(7) C(10) C(11) 119.8(4) . . . yes
C(9) C(10) C(11) 122.9(3) . . . yes
C(10) C(11) C(12) 120.2(3) . . . yes
C(5) C(12) C(11) 119.3(4) . . . yes
C(5) C(12) C(13) 119.8(3) . . . yes
C(11) C(12) C(13) 121.0(3) . . . yes
C(12) C(13) C(14) 119.0(3) . . . yes
S(1) C(14) C(3) 114.0(3) . . . yes
S(1) C(14) C(13) 124.3(3) . . . yes
C(3) C(14) C(13) 121.7(4) . . . yes
C(1) C(15) C(16) 121.8(4) . . . yes
C(1) C(15) C(20) 120.6(4) . . . yes
C(16) C(15) C(20) 117.6(4) . . . yes
C(15) C(16) C(17) 121.5(4) . . . yes
C(16) C(17) C(18) 120.1(5) . . . yes
C(17) C(18) C(19) 119.7(5) . . . yes
C(18) C(19) C(20) 120.6(5) . . . yes
C(15) C(20) C(19) 120.5(4) . . . yes
C(8) C(21) C(22) 121.7(4) . . . yes
C(8) C(21) C(26) 121.4(4) . . . yes
C(22) C(21) C(26) 116.9(4) . . . yes
C(21) C(22) C(23) 121.0(4) . . . yes
C(22) C(23) C(24) 120.9(5) . . . yes
C(23) C(24) C(25) 119.1(5) . . . yes
C(24) C(25) C(26) 121.3(5) . . . yes
C(21) C(26) C(25) 120.7(4) . . . yes
#------------------------------------------------------------------------------
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
S(1) C(1) C(2) C(3) -1.1(3) . . . . yes
S(1) C(1) C(15) C(16) 2.7(5) . . . . yes
S(1) C(1) C(15) C(20) -177.0(3) . . . . yes
S(1) C(14) C(3) C(2) 0.2(4) . . . . yes
S(1) C(14) C(3) C(4) 178.9(3) . . . . yes
S(1) C(14) C(13) C(12) -179.1(3) . . . . yes
S(2) C(7) C(6) C(5) 177.5(3) . . . . yes
S(2) C(7) C(10) C(9) -0.2(4) . . . . yes
S(2) C(7) C(10) C(11) -178.0(3) . . . . yes
S(2) C(8) C(9) C(10) 0.8(3) . . . . yes
S(2) C(8) C(21) C(22) -4.7(5) . . . . yes
S(2) C(8) C(21) C(26) 176.5(3) . . . . yes
C(1) S(1) C(14) C(3) -0.7(3) . . . . yes
C(1) S(1) C(14) C(13) 178.8(3) . . . . yes
C(1) C(2) C(3) C(4) -178.2(3) . . . . yes
C(1) C(2) C(3) C(14) 0.5(4) . . . . yes
C(1) C(15) C(16) C(17) 179.9(4) . . . . yes
C(1) C(15) C(20) C(19) 179.5(4) . . . . yes
C(2) C(1) S(1) C(14) 1.1(3) . . . . yes
C(2) C(1) C(15) C(16) -177.5(3) . . . . yes
C(2) C(1) C(15) C(20) 2.8(5) . . . . yes
C(2) C(3) C(4) C(5) 179.3(3) . . . . yes
C(2) C(3) C(14) C(13) -179.3(3) . . . . yes
C(3) C(2) C(1) C(15) 179.1(3) . . . . yes
C(3) C(4) C(5) C(6) 179.9(3) . . . . yes
C(3) C(4) C(5) C(12) -0.6(5) . . . . yes
C(3) C(14) C(13) C(12) 0.3(5) . . . . yes
C(4) C(3) C(14) C(13) -0.5(5) . . . . yes
C(4) C(5) C(6) C(7) -179.2(3) . . . . yes
C(4) C(5) C(12) C(11) 179.9(3) . . . . yes
C(4) C(5) C(12) C(13) 0.3(5) . . . . yes
C(5) C(4) C(3) C(14) 0.7(5) . . . . yes
C(5) C(6) C(7) C(10) -1.5(5) . . . . yes
C(5) C(12) C(11) C(10) 0.1(5) . . . . yes
C(5) C(12) C(13) C(14) -0.2(5) . . . . yes
C(6) C(5) C(12) C(11) -0.5(5) . . . . yes
C(6) C(5) C(12) C(13) 179.9(3) . . . . yes
C(6) C(7) S(2) C(8) -178.5(3) . . . . yes
C(6) C(7) C(10) C(9) 178.9(3) . . . . yes
C(6) C(7) C(10) C(11) 1.1(5) . . . . yes
C(7) S(2) C(8) C(9) -0.8(3) . . . . yes
C(7) S(2) C(8) C(21) 177.9(3) . . . . yes
C(7) C(6) C(5) C(12) 1.2(5) . . . . yes
C(7) C(10) C(9) C(8) -0.3(4) . . . . yes
C(7) C(10) C(11) C(12) -0.3(5) . . . . yes
C(8) S(2) C(7) C(10) 0.6(3) . . . . yes
C(8) C(9) C(10) C(11) 177.4(3) . . . . yes
C(8) C(21) C(22) C(23) 179.9(4) . . . . yes
C(8) C(21) C(26) C(25) -179.2(4) . . . . yes
C(9) C(8) C(21) C(22) 174.0(3) . . . . yes
C(9) C(8) C(21) C(26) -4.7(5) . . . . yes
C(9) C(10) C(11) C(12) -178.0(3) . . . . yes
C(10) C(9) C(8) C(21) -178.0(3) . . . . yes
C(10) C(11) C(12) C(13) 179.7(3) . . . . yes
C(11) C(12) C(13) C(14) -179.8(3) . . . . yes
C(14) S(1) C(1) C(15) -179.1(3) . . . . yes
C(15) C(16) C(17) C(18) 1.0(7) . . . . yes
C(15) C(20) C(19) C(18) 0.2(6) . . . . yes
C(16) C(15) C(20) C(19) -0.2(6) . . . . yes
C(16) C(17) C(18) C(19) -0.9(7) . . . . yes
C(17) C(16) C(15) C(20) -0.4(6) . . . . yes
C(17) C(18) C(19) C(20) 0.3(7) . . . . yes
C(21) C(22) C(23) C(24) -0.1(7) . . . . yes
C(21) C(26) C(25) C(24) -1.2(7) . . . . yes
C(22) C(21) C(26) C(25) 2.0(6) . . . . yes
C(22) C(23) C(24) C(25) 1.0(7) . . . . yes
C(23) C(22) C(21) C(26) -1.3(6) . . . . yes
C(23) C(24) C(25) C(26) -0.3(7) . . . . yes
C(23) C(24) C(25) C(26) -0.3(7) . . . . yes
#------------------------------------------------------------------------------
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_1
_geom_contact_site_symmetry_2
_geom_contact_publ_flag
S(1) C(8) 3.509(4) . 2_555 ?
S(2) C(1) 3.536(4) . 2_645 ?
C(15) C(26) 3.594(6) . 2_545 ?
#------------------------------------------------------------------------------
#------------------------------------------------------------------------------